Full Report Set



  ASAP 2020 V3.01 H    Unit 1    Serial #: 220    Page  1  

     Sample:    SJO-1242                     
   Operator:                                 
  Submitter:                                 
       File:    D:\DATA\DUMELE\SJO-1242.SMP  

            Started:    26.08.2021 10:31:32       Analysis Adsorptive:    N2                    
          Completed:    29.08.2021 22:54:01       Analysis Bath Temp.:    -195.725 C           
        Report Time:    29.08.2021 22:53:58        Thermal Correction:    No                    
        Sample Mass:    0.0346 g                      Warm Free Space:    16.4579 cm Measured  
    Cold Free Space:    50.3929 cm            Equilibration Interval:    45 s                  
  Low Pressure Dose:    0.5000 mmol/g                 Automatic Degas:    No                    







                      Isotherm Tabular Report

   Relative       Absolute      Quantity    Elapsed    Saturation   
   Pressure       Pressure      Adsorbed     Time       Pressure    
    (p/p)          (kPa)       (mmol/g)    (h:min)       (kPa)     
-----
  1.#QNAN0000      1.#QNAN00     1.#QNAN      00:58    101.7524141  
  0.000008999      0.0009158     0.50791      01:50      1.#QNAN00  
  0.000003755      0.0003822     1.01807      02:34      1.#QNAN00  
  0.000011412      0.0011618     1.52605      03:22      1.#QNAN00  
  0.000019096      0.0019444     2.02983      04:21      1.#QNAN00  
  0.000043580      0.0044387     2.52371      05:44      1.#QNAN00  
  0.000086955      0.0088625     3.00087      09:02      1.#QNAN00  
  0.000166940      0.0170219     3.44686      11:08      1.#QNAN00  
  0.000282918      0.0288635     3.84735      13:50      1.#QNAN00  
  0.000440410      0.0449600     4.20349      17:00      1.#QNAN00  
  0.000806769      0.0823898     4.69654      18:45      1.#QNAN00  
  0.001365043      0.1394518     5.17734      20:29      1.#QNAN00  
  0.002158743      0.2206113     5.64034      22:10      1.#QNAN00  
  0.003215567      0.3287188     6.07906      23:45      1.#QNAN00  
  0.004635295      0.4738957     6.49937      24:11      1.#QNAN00  
  0.006417164      0.6561500     6.89275      24:48      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      24:53    102.2509490  
  0.008455138      0.8643510     7.25171      25:21      1.#QNAN00  
  0.010572412      1.0807433     7.54633      25:27      1.#QNAN00  
  0.011839982      1.2102596     7.70216      25:33      1.#QNAN00  
  0.012249439      1.2520631     7.76073      25:38      1.#QNAN00  
  0.013551654      1.3851006     7.90166      25:44      1.#QNAN00  
  0.013904696      1.4211504     7.93900      25:47      1.#QNAN00  
  0.016230964      1.6588299     8.15586      25:53      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      25:55    102.1999197  
  0.017073590      1.7448553     8.24582      26:00      1.#QNAN00  
  0.018486314      1.8891609     8.36058      26:05      1.#QNAN00  
  0.020750746      2.1204751     8.53700      26:11      1.#QNAN00  
  0.023806190      2.4326328     8.74269      26:15      1.#QNAN00  
  0.026848614      2.7434218     8.93491      26:20      1.#QNAN00  
  0.030346163      3.1006913     9.13176      26:25      1.#QNAN00  
  0.033815752      3.4550776     9.30716      26:30      1.#QNAN00  
  0.034626733      3.5378604     9.35277      26:33      1.#QNAN00  
  0.040141993      4.1012112     9.59469      26:38      1.#QNAN00  
  0.044843192      4.5813529     9.77924      26:43      1.#QNAN00  
  0.051358418      5.2467804     9.99960      26:48      1.#QNAN00  
  0.052111621      5.3236103    10.03084      26:51      1.#QNAN00  
  0.052412982      5.3542784    10.04534      26:54      1.#QNAN00  
  0.053809728      5.4968830    10.08930      26:56      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      26:59    102.1518198  
  0.054796127      5.5975258    10.12658      27:02      1.#QNAN00  
  0.055706143      5.6904874    10.15534      27:05      1.#QNAN00  
  0.057092502      5.8321084    10.19186      27:08      1.#QNAN00  
  0.058401869      5.9658646    10.23122      27:11      1.#QNAN00  
  0.059876430      6.1164952    10.26876      27:13      1.#QNAN00  
  0.061540633      6.2864987    10.30929      27:16      1.#QNAN00  
  0.063328685      6.4691538    10.35397      27:19      1.#QNAN00  
  0.065201658      6.6604839    10.39579      27:22      1.#QNAN00  
  0.067175715      6.8621407    10.44510      27:26      1.#QNAN00  
  0.068939952      7.0423627    10.48025      27:28      1.#QNAN00  
  0.071112246      7.2642694    10.52308      27:31      1.#QNAN00  
  0.073228221      7.4804224    10.56571      27:33      1.#QNAN00  
  0.075596155      7.7223144    10.61136      27:36      1.#QNAN00  
  0.080124297      8.1848767    10.69571      27:39      1.#QNAN00  
  0.086130376      8.7984148    10.79488      27:43      1.#QNAN00  
  0.097645160      9.9746794    10.96054      27:46      1.#QNAN00  
  0.100230433     10.2387742    11.00194      27:49      1.#QNAN00  
  0.111368767     11.3765847    11.13844      27:52      1.#QNAN00  
  0.126778078     12.9506866    11.30953      27:55      1.#QNAN00  
  0.141158715     14.4197078    11.44969      27:58      1.#QNAN00  
  0.144064114     14.7165045    11.48050      28:00      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      28:02    102.1524871  
  0.164023968     16.7557487    11.65373      28:06      1.#QNAN00  
  0.187047177     19.1079179    11.82415      28:09      1.#QNAN00  
  0.212673718     21.7260971    12.00085      28:12      1.#QNAN00  
  0.241701985     24.6918594    12.18172      28:15      1.#QNAN00  
  0.252059867     25.7503399    12.24990      28:18      1.#QNAN00  
  0.275487987     28.1439933    12.38165      28:20      1.#QNAN00  
  0.300747456     30.7249157    12.52440      28:23      1.#QNAN00  
  0.313355726     32.0134188    12.59871      28:26      1.#QNAN00  
  0.350506183     35.8091402    12.78106      28:28      1.#QNAN00  
  0.373573506     38.1662915    12.89761      28:31      1.#QNAN00  
  0.400288844     40.8960318    13.02780      28:33      1.#QNAN00  
  0.404134421     41.2894607    13.06088      28:36      1.#QNAN00  
  0.450097528     45.9858041    13.27016      28:38      1.#QNAN00  
  0.477923261     48.8293575    13.41355      28:41      1.#QNAN00  
  0.500408587     51.1271264    13.51949      28:43      1.#QNAN00  
  0.523320970     53.4685685    13.63482      28:45      1.#QNAN00  
  0.550364953     56.2324328    13.77094      28:48      1.#QNAN00  
  0.595526402     60.8472440    14.00590      28:50      1.#QNAN00  
  0.599995198     61.3046406    14.04810      28:53      1.#QNAN00  
  0.650759199     66.4923336    14.32279      28:56      1.#QNAN00  
  0.694512199     70.9637931    14.59696      28:59      1.#QNAN00  
  0.700270127     71.5527504    14.65984      29:01      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      29:04    102.1801215  
  0.741004442     75.7165284    14.96686      29:07      1.#QNAN00  
  0.772566584     78.9422078    15.24136      29:10      1.#QNAN00  
  0.807486050     82.5109988    15.60222      29:13      1.#QNAN00  
  0.871536156     89.0567511    16.59724      29:17      1.#QNAN00  
  0.913469808     93.3431753    17.80058      29:23      1.#QNAN00  
  0.927127167     94.7397649    18.43204      29:27      1.#QNAN00  
  0.946805190     96.7523928    19.73644      29:34      1.#QNAN00  
  0.953777492     97.4661770    20.45485      29:39      1.#QNAN00  
  0.992818056    101.4603075    28.56093      29:56      1.#QNAN00  
  0.994719475    101.6554331    31.56007      29:59      1.#QNAN00  
  0.987566700    100.9252602    29.41750      30:02      1.#QNAN00  
  0.976767775     99.8229825    28.24321      30:07      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      30:09    102.1977959  
  0.969196281     99.0513010    26.51794      30:17      1.#QNAN00  
  0.965466945     98.6713435    25.67007      30:23      1.#QNAN00  
  0.964044796     98.5267834    25.33749      30:27      1.#QNAN00  
  0.958460539     97.9574291    24.19092      30:34      1.#QNAN00  
  0.953064801     97.4071324    23.24667      30:40      1.#QNAN00  
  0.947481160     96.8378106    22.31785      30:47      1.#QNAN00  
  0.939007279     95.9730703    21.25673      30:54      1.#QNAN00  
  0.934277761     95.4906310    20.71321      30:59      1.#QNAN00  
  0.924162941     94.4579439    19.85315      31:05      1.#QNAN00  
  0.915866892     93.6109431    19.28161      31:10      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      31:13    102.2108156  
  0.905219381     92.5251434    18.69674      31:17      1.#QNAN00  
  0.890316064     91.0042070    18.05815      31:22      1.#QNAN00  
  0.875335781     89.4748565    17.57013      31:26      1.#QNAN00  
  0.860591121     87.9695274    17.18484      31:30      1.#QNAN00  
  0.840172543     85.8836878    16.76434      31:33      1.#QNAN00  
  0.820413661     83.8656566    16.42425      31:37      1.#QNAN00  
  0.800219026     81.8025690    16.13707      31:40      1.#QNAN00  
  0.770305269     78.7458616    15.79427      31:43      1.#QNAN00  
  0.740310859     75.6808135    15.51052      31:46      1.#QNAN00  
  0.700381112     71.5999796    15.18536      31:49      1.#QNAN00  
  0.650142865     66.4651630    14.84420      31:52      1.#QNAN00  
  0.600308150     61.3714401    14.56096      31:55      1.#QNAN00  
  0.550580380     56.2884911    14.29608      31:58      1.#QNAN00  
  0.500157406     51.1343076    14.04795      32:01      1.#QNAN00  
  0.451353198     46.1457030    13.68125      32:05      1.#QNAN00  
  0.398245926     40.7167293    13.41071      32:08      1.#QNAN00  
  0.351043258     35.8912827    13.18940      32:11      1.#QNAN00  
  0.300505179     30.7246614    12.94060      32:14      1.#QNAN00  
  1.#QNAN0000      1.#QNAN00     1.#QNAN      32:17    102.2449681  
  0.250367426     25.5993370    12.66685      32:20      1.#QNAN00  
  0.200302180     20.4807342    12.35975      32:23      1.#QNAN00  
  0.150626950     15.4019057    11.98219      32:27      1.#QNAN00  
  0.101012455     10.3290795    11.44203      32:32      1.#QNAN00  
  0.070472463      7.2064942    10.92700      32:38      1.#QNAN00  


 Options Report


              Sample Tube

         Warm freespace:    1.0000 cm  
         Cold freespace:    1.0000 cm  
    Non-ideality factor:    0.0000620   
  Use Isothermal Jacket:    Yes         
         Use Filler Rod:    Yes         
       Vacuum seal type:    Seal Frit   

 Analysis Conditions


                 Preparation

               Fast evacuation:    No        
  Unrestricted evacuation from:    0.67 kPa  
               Vacuum setpoint:    1.3 Pa    
               Evacuation time:    0.10 h    
                     Leak test:    No        
                 Use TransSeal:    No        

                Free Space

             Free-space type:    Measured  
  Lower dewar for evacuation:    Yes       
             Evacuation time:    0.10 h    
                 Outgas test:    No        

                                                       p and Temperature

         p and T type:    Measure p at intervals during analysis.  Calculate the Analysis Bath Temperature from these values.  
  Measurement interval:    60 min                                                                                                

                         Dosing

  Use first pressure fixed dose:    No                  
   Use maximum volume increment:    No                  
               Target tolerance:    5.0% or 0.6666 kPa  
            Low pressure dosing:    Yes                 
                    Dose amount:    0.50000 mmol/g      
    Minimum equilibration delay:    0.00 h              
    Maximum equilibration delay:    999.00 h            

                      Equilibration

       Equilibration time (p/p = 0.010000000):    45 s   
       Equilibration time (p/p = 1.000000000):    10 s   
  Minimum equilibration delay at p/p >= 0.995:    600 s  

             Sample Backfill

  Backfill at start of analysis:    Yes  
    Backfill at end of analysis:    Yes  
                   Backfill gas:    N2   

                Adsorptive Properties

                         Adsorptive:    Nitrogen     
          Maximum manifold pressure:    123.323 kPa  
                Non-ideality factor:    0.0000620    
          Density conversion factor:    0.0015468    
  Therm. tran. hard-sphere diameter:    3.860       
     Molecular cross-sectional area:    0.162 nm    


  Inside diameter of sample tube:    9.53 mm  

